HIGH TEMPERATURE ELASTIC STRAIN EVOLUTION IN Si3N4-BASED CERAMICS

نویسندگان

  • G. A. Swift
  • E. Ustundag
  • B. Clausen
  • M.A.M. Bourke
  • H.-T. Lin
  • C.-W. Li
چکیده

Tension experiments in vacuum were performed on a monolithic Si3N4 sample at 1375°C and a 20Vol% SiCp-Si3N4 composite sample at 1400°C using the new SMARTS diffractometer at the Los Alamos Neutron Science Center. The deep penetration of neutrons facilitated these in-situ studies. In particular, the hkl-dependent strains were measured and the results interpreted by Eshelby-based modeling for the Si3N4-SiCp sample. The diffraction data also provided information about thermal expansion coefficients for both specimens and the elastic constants at high temperature for the monolithic sample.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Microstructure of Spark Plasma-Sintered Silicon Nitride Ceramics

The microstructure and phase composition of the high-content Al2O3-Y2O3-doped spark plasma-sintered silicon nitride were investigated. Fully dense silicon nitride ceramics with a typical α-Si3N4 equiaxed structure with average grain size from 200 to 530 nm, high elastic modulus of 288 GPa, and high hardness of 2038 HV were spark plasma sintered (SPSed) at 1550 °C. Silicon nitride with elongated...

متن کامل

Pressureless Sintering of Si3N4 Ceramic Using AlN and Rare-Earth Oxides

Using intermediate, liquid-forming compositions in the approach focuses on the Si3N4–R2O3 binary, where R2O3 is any (Y,La)2O3–AlN system as additives, fully dense Si3N4 ceramrare-earth oxide (or Y2O3) used singly or severally. After sinics with high strength at high temperature have been tering, this composition forms -Si3N4 and some refractory rareobtained by pressureless sintering. The cerami...

متن کامل

Effect of Sintering Aid Composition on the Processing of Si3N4/BN Fibrous Monolithic Ceramics

Si3N4/BN fibrous monoliths were prepared with 4 wt% Y2O3 added as a sintering aid to the Si3N4. Residual carbon, present in the billet before hot-pressing, was shown to influence the final microstructure. The sintering aid glass, known to migrate into the BN cell boundaries during hotpressing, was not sufficient in quantity to prevent premature shear failure when samples were tested in flexure....

متن کامل

High Precision Temperature Insensitive Strain Sensor Based on Fiber-Optic Delay

A fiber-optic delay based strain sensor with high precision and temperature insensitivity was reported, which works on detecting the delay induced by strain instead of spectrum. In order to analyze the working principle of this sensor, the elastic property of fiber-optic delay was theoretically researched and the elastic coefficient was measured as 3.78 ps/km·με. In this sensor, an extra refere...

متن کامل

Potential use of only Yb2O3 in producing dense Si3N4 ceramics with high thermal conductivity by gas pressure sintering.

Yb2O3 is an efficient sintering additive for enhancing not only thermal conductivity but also the high-temperature mechanical properties of Si3N4 ceramics. Here we report the fabrication of dense Si3N4 ceramics with high thermal conductivity by the gas pressure sintering of α-Si3N4 powder compacts, using only Yb2O3 as an additive, at 1900 °C under a nitrogen pressure of 1 MPa. The effects of Yb...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:

دوره   شماره 

صفحات  -

تاریخ انتشار 2002